Electron microprobes

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  • Electron Microprobes
definition
  • An electron microprobe is an electron microscope designed for the non-destructive x-ray microanalysis and imaging of solid materials. It is capable of high spatial resolution and relatively high analytical sensitivity. [Source: Caltech]
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Abstract from DBPedia
    An electron microprobe (EMP), also known as an electron probe microanalyzer (EPMA) or electron micro probe analyzer (EMPA), is an analytical tool used to non-destructively determine the chemical composition of small volumes of solid materials. It works similarly to a scanning electron microscope: the sample is bombarded with an electron beam, emitting x-rays at wavelengths characteristic to the elements being analyzed. This enables the abundances of elements present within small sample volumes (typically 10-30 cubic micrometers or less) to be determined, when a conventional accelerating voltage of 15-20 kV is used. The concentrations of elements from lithium to plutonium may be measured at levels as low as 100 parts per million (ppm), material dependent, although with care, levels below 10 ppm are possible. The ability to quantify lithium by EPMA became a reality in 2008.

    電子線マイクロアナライザ(でんしせんマイクロアナライザ、英: Electron Probe Micro Analyzer)または電子プローブ微小分析器、略称 EPMAとは電子線を対象物に照射する事により発生する特性X線の波長と強度から構成元素を分析する電子マイクロプローブ(EMP)装置の一つである。二次電子像や反射電子像による観察が主体の電子顕微鏡に特性X線検出器としてエネルギー分散型X線分析(EDS)を付加したもの(分析用のSEMやTEM、など)と比較して、EPMAは元素分析を主体としたものであり、特性X線検出器に波長分散型X線分析(WDS)を用いるために定量精度は良いが検出効率が悪く、より高い照射電流を必要とする。 10~30立方マイクロメータの試料があればホウ素からプルトニウムまで100(ppm)を下限とする検出感度で定量的に分析出来る。

    (Source: http://dbpedia.org/resource/Electron_microprobe)